Last Updated on March 8, 2023 by
For different chemical reactions and other applications, pressure reactors are used. Various chemical reactions like hydrogenation, polymerization, catalyst screening, and corrosion testing are the most common jobs that pressure reactors can perform. However, when it comes to Lab Scale High-Pressure Stainless Steel Reactor, they are low-capacity plants, but they provide high flexibility facilities.
Usually, they are used at the initial research stage, when you don’t need high production capacity. Instead great amount of experimental essays is needed. On a laboratory scale high-pressure stainless steel reactor, any modifications could be done quickly and with a relatively very low amount. It will allow you to reach the best process configuration and conditions easily. In addition, many companies use high-pressure stirred reactor autoclave to cure composite materials. In this way, it can be possible to apply a thermal cycle.
Lab Scale High-Pressure Stainless Steel Reactor for Batch Hydrogenation Reaction
This apparatus consists of a stainless-steel high-pressure reactor with an internal volume of 25 cm3. However, a magnetic stirrer was also disposed of in the reactor, and PID was controlled. A thermostatic oil bath can control the reaction temperature. A nitrogen supply ensures an inert atmosphere inside the reactor as a safety stage before and after hydrogen feeding.
Therefore, a higher reactor could be used with a total volume of 170 ml. Using Broncho’s mass flow controllers, the nitrogen and hydrogen are fed until reacting pressure is reached. A mixture of hydrogen and nitrogen or pure hydrogen could be used for hydrogenation.
Use of Lab Scale High-Pressure Stainless Steel Reactor
It is commonly used for chemistry and chemical engineering synthetic reactions under very high temperatures and pressure or catalytic reaction. This type of environmental condition requires measuring the pressure, temperature and speeding at the same time. They add inert gas protection, soothe pressure and realize online sampling or feeding. Moreover, they are widely used for flammable and explosive, highly toxic, precious media and other highly porous chemical mediums for stirring reactions. Using the vulcanization process and fluoridation of petroleum, chemical, organic synthesis, polymer polymerization, Hydrogenation, and other important non-leakage reactions can perform through a high-pressure stirred reactor autoclave.la
Parts of Lab Scale High-Pressure Stainless Steel Reactor
There are some most important parts of the Lab Scale High-Pressure Reactor. Without those parts, it can’t work properly, and the results would not be 100%.
Brushless Motor
It can control digital frequency conversion. Strong controllability, low noise, smooth operation, and no need for daily maintenance are the most important jobs of the motor of Lab Scale High-Pressure Stainless Steel Reactor. The maximum speed of the brushless motor of this reactor is 1350rpm.
Looking Glass
A looking glass in Lab Scale High-Pressure Reactor is used to observe the change of the reaction medium in the vessel. It has a high light transmittance and acid as well as alkali resistance. It is just a safety accessory and should be checked regularly.
Vessel Lid
The vessel lid is equipped with standard ports, including a sight glass port, feed port, thermometer port, vacuum instrument port, constant pressure funnel port and air guide port.
Controller
It is the most important part of the high-pressure stirred reactor autoclave. It adopts variable frequency speed regulation. However, vacuum coating is used to protect the internal components of the variable frequency. This vacuum coating is corrosion-resistant.
Lab Scale High-Pressure Reactor for Batch Hydrothermal Hydrolysis
The stainless steel lab-scale high-pressure reactor can contain a total volume of 300 ml. Moreover, it can operate up to 227bar at 454°C. The inner of the vessel is equipped with a DispersimaxTM turbine stirrer, a baffle bar and a cooling coil. The high-pressure stirred reactor autoclave is coupled with the ceramic band heater and the pressure gauge. Inside the temperature, there is IB50 apparatus that controls the furnace temperature and stirring speed.
It is used for biomass hydrolysis. However, it can be operated continuously, but its current use is semi-continuous. The reactor is heated to the desired temperature, and the current liquid pours into it. After the time is over, the process of refrigeration is performed from the inside as well as the outside. The cooling coil cools it down, and the cold bath works for the outside.
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Conclusion
The high-pressure lab-scale reactor system is designed to use metal pressure vessels. The high-pressure stirred reactor autoclave or Lab Scale High-Pressure Reactor ensures high corrosion resistance, and safety features guarantee safe reactions under pressure.
Apart from this if you’re interested to know about 6 Things to Check When Looking for Manufacturing Companies That Make Stainless Steel Tubes then you can visit our Tech category.
